Primer: Distillation

The Primer can be downloaded here. It is a .pdf file priced at $25 (U.S.).

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Summary

Distillation remains the backbone of chemical and energy processing, separating complex mixtures into valuable products.

Distillation: A Primer explains the principles, design, and operation of both batch and continuous systems — from moonshine stills to refinery towers. The Primer covers column internals, reboilers, reflux control, and advanced methods such as azeotropic and extractive distillation. The Primer also addresses economics, safety, and environmental management, referencing key industry standards.

Written for engineers, operators, and technical professionals, it combines practical insight with clear explanation.

The Primer concludes with a 10-question quiz, making this an ideal resource for training and professional development in process operations.

Table of Contents

Introduction    
Principles of Distillation    
Batch Distillation
   Specialty and Fine Chemicals    
   Pharmaceutical Manufacturing   
   Solvent Recovery    
   Research Applications   
Continuous Distillation   
   Feed Composition   
   Reflux and Reflux Ratio    
Close-Boiling Separations
   Azeotropic Distillation   
   Extractive Distillation    
Reboilers    
   Thermosyphon Reboiler   
   Kettle Reboiler    
   Forced Circulation Reboiler   
Column Internals   
   Trays (Plates)    
   Packing    
Operations
   Startup    
   Steady-State Operation   
   Shutdown    
   Operational Challenges    
Economics of Distillation   
Safety and Environmental 
Standards and Best Practices  
Conclusion  
Knowledge Check: 10-Question Quiz